Forschungspublikationen

3 Ergebnisse
28.01.2026

Real-time monitoring system for textile membranes

Gewebe Sensorik Technische Textilien Smart Textiles Tests

Zusammenfassung

In the IGF project 01IF22600N, a real-time, fiber sensor-based monitoring system for textile membranes was developed at the ITM of TU Dresden. Textile membrane structures are used in numerous technical applications, but methods for continuous, full-area condition monitoring have been lacking until now. The project goal was to implement an integrated sensor system that detects the global stress state of the membrane and thus provides indications of overloads and damage. To this end, suitable thread-like sensor materials were identified, sensor structures were integrated into the membrane using embroidery and weaving techniques, and robust contacting and coating strategies were developed. Based on experimental data and FEM simulations, an AI-based regression model was developed that determines load positions in real time with an accuracy of ±3 mm and load amounts with ±0.6 N, and uses this information to derive the full-surface stress state. The results show that the mechanical performance of the membrane is largely maintained despite sensor integration and that textile structures can be effectively expanded into intelligent, self-monitoring support structures.

Bericht

Introduction

Textile membrane structures have established themselves as lightweight, flexible, and yet high-performance components in numerous technical applications, such as architectural roof and facade systems, mobile and stationary protective structures, and maritime environments. However, their load-bearing capacity and fatigue strength depend crucially on static and dynamic stresses, as local overloads and undetected damage can lead to sudden structural failure in extreme cases. In practice, inspections have so far been based predominantly on visual checks and selective measurements, which do not allow for continuous condition monitoring or comprehensive evaluation of membrane behavior and are therefore of limited value for predictive maintenance. Against this background, the IGF project 01IF22600N aims to transform textile membranes into intelligent, sensor-functionalized structures that record their own stress and damage status in real time. To this end, a textile sensor structure [1] is integrated into the membrane structure [2, 3] and its measured values are evaluated in combination with simulation results [4, 5] using AI-based algorithms [6].

Objective

The central goal of the project was to create a fiber sensor-based monitoring system that determines the full-surface stress distribution of textile membranes and can thus provide indications of fatigue and structural damage. To this end, thread-like sensor materials were examined for their elongation properties and suitability for use in combination with the membrane. Using the preferred variants, weaving patterns for fabrics with integrated sensor and energy supply structures were developed and manufactured. These patterns were mechanically characterized while simultaneously recording the sensor measurements. At the same time, the global strain distribution was simulated for the test scenarios. Based on this data, algorithms were developed that calculate the global strain distribution from the sensor measurements and output it in real time, e.g., as a heat map. The developed system was successfully implemented and integrated into a functional demonstrator.

Results

Thread-shaped sensor materials

Silver-coated polyamide yarns, pseudoelastic shape memory alloys (SMA), and precision resistance alloys were selected as promising options in the search for a suitable thread sensor material. The behavior of the electrical resistance under tension, the temperature stability, and the suitability for subsequent textile integration into the membrane composite were investigated. Cyclic tensile tests up to 10 % strain were chosen as the characterization method and were repeated at various temperatures between -20 °C and 70 °C. As a result of these investigations, SMAs proved unsuitable due to their high temperature dependence and strongly non-linear resistance behavior. Both precision resistance alloys (Isaohm® / Isabellenhütte) and silver-coated polyamide yarns (SilverTech+® 150 / Amann & Söhne GmbH & Co. KG) appeared to be fundamentally suitable and were taken into account in the following tests, with precision resistance alloys being identified as the preferred option due to their lower temperature dependence and linear sensor behavior. A fine wire (LitzWire / Rudolf Pack GmbH & Co. KG) was selected for the implementation of the electrical contact network due to its good textile processability and low basic electrical resistance (<< 1 Ω/m).

Development and production of functional samples

Two approaches were pursued for the development of a functional sample. On the one hand, samples were produced using embroidery technology and the TFP process; on the other hand, the thread-like sensor and the textile feed line were already integrated into the semi-finished textile product during the weaving process. For the embroidered samples, a commercially available membrane (HEYtex tentorium 900) was used. Both the silver-coated polyamide yarn and the precision resistance alloy were applied in patches using the tailored fiber placement (TFP) process (Figure 1) in order to increase the sensor length and thus improve measurement accuracy. In addition, the sensor patches were applied in different orientations in order to detect stretching in different directions. At the same time, the silver-coated polyamide yarn Shieldex® 117, which is more robust in textile processing than SilverTech+® 150, was embroidered using regular zigzag and chain stitches without auxiliary thread.

For the woven patterns, a grid with weft and warp threads made of feedline and sensor material was designed, which was combined with the polyester base fabric in terms of pattern (Figure 2). This made it possible to create arrangements with sensors in the warp and weft directions, which later allowed the calculation of tensile stress in different directions. A total of three patterns were created, which differed in terms of the length and position of the sensors. The third variant was a hybrid that combined a woven supply network with sensor patches that were embroidered on afterwards. Two types of intersection points, with and without electrical contact, were created in the conductive structures and implemented using binding techniques. The samples were produced on a gripper loom with center transfer (Lindauer Dornier P1).

A key development step was the creation of practical contacting strategies for the sensor network. Conventional soldering methods caused damage to the textile base material due to high process temperatures, while alternative conductive adhesives initially exhibited excessive contact resistance in the kΩ range. However, by using an epoxy-silver conductive adhesive (8330S) with defined curing (160°C, 90 s, light pressure), stable, low-resistance contacts could be achieved both within the fabric and at the edges of the goods; in combination with crimp contacts, a mechanically robust and electrically reliable connection to external measurement technology was achieved.

Coating of the textile semi-finished product with integrated sensor structure

The functionalized fabrics were then coated with a PVC paste (plus 5% bonding agent) provided by the industry partner using a LineCoater from COATEMA (Figure 3). It was found that both integrally woven (0.2 mm) and embroidered sensor and supply structures (0.7 mm) could be integrated into the membrane with a low application thickness, so that the basic mechanical properties of the membrane were only minimally altered, while complete coverage and electrical insulation of the sensor technology was achieved. Additional tests with transfer foils and directly applied PVC adhesive layers showed that manual or semi-manual coating strategies are also suitable for local or subsequent functionalization, especially for smaller membrane areas.

Characterization of the membrane with integrated sensor technology

The manufactured samples were first tested in uniaxial tensile tests. In addition to the basic mechanical properties, the electromechanical properties were also determined. Particular attention was paid to the influence of the integrated sensor technology on structural integrity. Tests were carried out in both the weft and warp directions. With a maximum force of 3810 N at 23.2 % elongation in the weft direction and 4100 N at 24.9 % elongation in the warp direction, the manufactured samples were at a similar level to the commercial product from Heytex (weft: 3780 N at 25.8 %; warp: 3920 N at 20.6 %). Accordingly, it was not expected that the mechanical performance would be affected by the integration of the sensor network.

Development of algorithms for full-surface strain state detection

Based on biaxial tensile tests of the commercial membrane, FE models were created for the full-surface simulation of stress conditions. In addition to providing a database for algorithm development, this also supported the selection of suitable sensor layouts. The modeling was based on shell elements with an anisotropic material model. Based on the calibrated material model, simulations were performed with randomly varied load positions and magnitudes, which formed part of the database for algorithm development.

The AI model underlying the algorithms was based on a regressive model. To this end, the previously simulated load cases were applied to the demonstrator. The resulting sensor measurements were used to train the model. The model was then evaluated using the parameters mean absolute error (MAE), root mean squared error (RMSE), and coefficient of determination (R²). For the functional demonstrator, which consisted of a square, flat membrane, high accuracy was demonstrated for position determination in the single-digit mm range. The amount of load was also determined precisely with a coefficient of determination of 0.9604. The system achieves ± 3 mm spatial resolution and ± 0.6 N force accuracy for demonstrator loads < 50 N and is scalable up to kN load ranges. Based on the determined values for the position and magnitude of a load application, the corresponding full-area stress state was determined using multi-stage k-nearest neighbor models. The resulting model showed a high regression quality with a deviation of less than 5% from the FEM reference. In addition, the model proved to be very stable in general and allowed the desired real-time determination of the stress distribution. For the functional demonstrator, the results of the model were visualized in real time on a display unit next to the membrane (Figure 4), so that the effect of applied loads was immediately apparent to the user.

Conclusion

In summary, the IGF MeMo project shows that PVC-coated PES membranes can be further developed into intelligent, real-time capable support structures by combining suitable sensor materials, textile integration strategies, and robust contacting and coating processes. The experimental results prove that the mechanical performance of the membrane is largely retained despite the integration of the sensor technology and that the functional requirements – in particular with regard to the measuring range, temperature stability, and long-term behavior of the selected sensor materials – are met. The project developed an AI-based regression approach that determines load positions and amounts in real time from textile-integrated sensor signals and derives full-surface stress states from them without requiring numerical simulations during operation. The approach is characterized by high robustness against sensor-related scatter and low requirements for computing power and training data. The underlying methodology is fundamentally transferable to other large-area, deformable structures with integrated sensor technology, for example in textile architecture, lightweight construction, or membrane- and composite-based structural systems, e.g., in the maritime sector.

At the same time, the investigations clearly show that the type of integration and contacting has a significant influence on the quality of the sensor signals: Inline-contacted, integrally woven sensors are technologically sophisticated and currently still limited in terms of signal stability, while embroidered sensor networks with clearly defined, easily accessible contact points deliver significantly more robust and easier-to-evaluate signals. Thus, the work not only provides a complete technical toolkit, but also a clear preference for further system development towards embroidered, hybrid membrane solutions.

In the field of mechanical and electromechanical characterization, it seems sensible to expand biaxial testing programs on functionalized membranes. This would allow for an even closer link between experimental and numerical data and extend the validation of the material and damage descriptions used in the FEM models to the sensor membrane system as a whole. At the same time, the algorithms for load localization and stress reconstruction based on the data available to date can be expanded to include additional load collectives, more complex boundary conditions, and additional failure patterns, so that the monitoring system will continue to operate reliably in the long term, even in highly variable application scenarios.

On this basis, manufacturing and retrofitting concepts can be developed with a view to implementing intelligent, self-monitoring membrane structures in various industries - from construction and protective and safety applications to the maritime sector.

Acknowledgement

The IGF project 01IF22600N of the research association Forschungskuratorium Textil e.V., Reinhardtstr. 12-14, 10117 Berlin, was funded by the German Federal Ministry for Economic Affairs and Energy via the German Aerospace Center (DLR) as part of the program for the promotion of Industrial Collective Research (IGF) based on a resolution of the German Bundestag.

The authors would like to thank the aforementioned institutions for providing the financial resources. The research report and further information are available from the Institute of Textile Machinery and High Performance Material Technology at TU Dresden.

References

[1]   J. Mersch, C. A. G. Cuaran, A. Vasilev, A. Nocke, C. Cherif, and G. Gerlach, "Stretchable and Compliant Textile Strain Sensors," IEEE Sensors J., vol. 21, no. 22, pp. 25632–25640, 2021, doi: 10.1109/JSEN.2021.3115973.

[2]   K. Bremer, F. Weigand, Y. Zheng, L. S. Alwis, R. Helbig, and B. Roth, "Structural Health Monitoring Using Textile Reinforcement Structures with Integrated Optical Fiber Sensors," Sensors (Basel, Switzerland), vol. 17, no. 2, 2017, doi: 10.3390/s17020345.

[3]   E. Haentzsche, R. Mueller, T. Ruder, A. Nocke, and C. Cherif, "Integrative Manufacturing of Textile-Based Sensors for Spatially Resolved Structural Health Monitoring Tasks of Large-Scaled Composite Components," MSF, 825-826, pp. 571–578, 2015, doi: 10.4028/www.scientific.net/MSF.825-826.571.

[4]   T. D. Dinh et al., "A study of tension fabric membrane structures under in-plane loading: Nonlinear finite element analysis and validation," Composite Structures, vol. 128, pp. 10–20, 2015, doi: 10.1016/j.compstruct.2015.03.055.

[5]   T. D. Dinh, A. Rezaei, L. de Laet, M. Mollaert, D. van Hemelrijck, and W. van Paepegem, "A new elasto-plastic material model for coated fabric," Engineering Structures, vol. 71, pp. 222–233, 2014, doi: 10.1016/j.engstruct.2014.04.027.

[6]   J. Vitola, F. Pozo, D. A. Tibaduiza, and M. Anaya, "A Sensor Data Fusion System Based on k-Nearest Neighbor Pattern Classification for Structural Health Monitoring Applications," Sensors (Basel, Switzerland), vol. 17, no. 2, 2017, doi: 10.3390/s17020417.

 

AutorInnen: Karl Kopelmann Anna Happel Florian Schmidt Tobias Lang Hung Le Xuan Chokri Cherif

Technische Universität Dresden

Fakultät Maschinenwesen

Institut für Textilmaschinen und Textile Hochleistungswerkstofftechnik (ITM)

01062 Dresden

 

https://tu-dresden.de/ing/maschinenwesen/itm

More entries from TU Dresden, Institut für Textilmaschinen und Textile Hochleistungswerkstofftechnik ITM

06.03.2023

Technology Development for the Sustainable Production of High-purity Chitosan Filament Yarns with High Performance and Functionality (Chion)

Rohstoffe Fasern Garne Nachhaltigkeit

Zusammenfassung

In the IGF project 21168 BR ‘Chion’, a technology for the manufacturing of chitosan multifilament yarns from ionic liquids was developed, enabling the tailoring of the yarn properties regarding their performance and functionality in all process stages. The material costs, the field of application and the functionalities achievable by the multifilament yarns are defined by the raw material selection. By using ionic liquids, it was possible for the first time to process lower-cost chitosans in various qualities and degree of deacetylation < 90%, previously unavailable with conventional spinning processes. From the achieved and extensively evaluated project results, required process parameters for the successful transfer of the elaborated fundamentals to a pilot scale as well as the process development for the spinning of chitosan multifilament yarns with high performance and strengths up to 28 cN/tex on a pilot solvent wet spinning plant were derived and implemented. To demonstrate the textile processability of the multifilament yarns, textile demonstrators were successfully fabricated for the first time in conventional textile weaving, knitting or braiding processes on standard industrial textile machines.

Bericht

Introduction and Objective

In the 21st century, society's high level of interest in using products that are manufactured in a sustainable way and minimize environmental impact grows constantly. In this context, the textile and fiber industry has the opportunity to accelerate the development of organic products from renewable raw materials, such as chitin and chitosan, in order to respond to the social, national and international demand for organic products.

The biopolymer chitin and its derivative chitosan are versatile and well-known materials used in (bio-)medicine and pharmacy. However, they are rarely available as a pure textile product. Chitin is the second abundant biopolymer after cellulose with 1.5-105 t/a [1]. The semi-crystalline structure and stable network of molecular bonds limit the solubility of chitin significantly. Therefore, chitin derivative chitosan is being primarily addressed by research and material development. The chitosan class of materials demonstrates excellent biological and antibacterial properties as well as cell colonizability and biodegradability [2, 3]. In the last few years, considerable research efforts have been made to develop efficient chitosan products; nevertheless, the availability of pure chitosan multifilament yarns with long-term stability is currently extremely limited [4]. Likewise, a robust, scalable process for manufacturing of high-performance chitosan filament yarns is urgently needed, as current products are severely limited in terms of mechanical properties. Due to the natural provenance and variability of raw material properties, such as degree of deacetylation (DD), molecular weight (Mw), etc. There are still major challenges in producing of chitosan multifilament yarns using the acid- and alkali-dominated manufacturing processes established so far.

The aim of the IGF research project ‘Chion’ (21168 BR) was therefore to develop a robust wet-spinning process based on ionic solvents for manufacturing of multifilament yarns from 100 % chitosan with high performance and functionality.

Obtained Results

By using ionic liquids (IL), lower cost chitosans with lower Mw and DD < 90% became accessible to the wet-spinning process for the first time. A high content of acetamide groups in chitosan with low DD (< 90%) leads to the increase of intermolecular interactions, which resulted in improved mechanical performance with tensile strengths up to 28 cN/tex and proper textile processing of chitosan multifilament yarns. The extensive research of chitosan-IL-systems with different chitosan proveniences, Mw and DD 60 – 90% with imidazol-based IL was initially carried out on a laboratory scale for monofilaments. Based on the results, important process parameters and promising chitosan-IL combinations were obtained and the developed process was successfully transferred to the multifilament scale. A structural-mechanical adjustment of the properties of the chitosan multifilament yarns was a fundamental object of the research work: Each development step was systematically monitored by material and process characterizations and analyses. Further investigations included the solubility of chitosan in IL, viscosity studies, fiber morphology and geometry, chemical and physical material properties, crystallinity and degradation behavior, as well as on the influence of controlled fiber drawing during the spinning process according the adjustment of the textile-physical properties. By integrating acid- and temperature-sensitive agents into the spinning dope, the functionality of the chitosan multifilament yarns was demonstrated. As a result of the precise tailoring of the molecular fiber properties and the developed spinning process parameters, a robust, scalable wet-spinning process is now available for manufacturing of pure chitosan multifilament yarns in pilot scale. Finally, the textile processability of the chitosan multifilament yarns was investigated and demonstrated by knitting, weaving and braiding processes.

Investigation of the solubility of chitosan in IL and spinning dope preparation

Initially, the dissolving ability of IL for chitosan was investigated and evaluated. Through systematic experiments, 19 commercially available chitosan materials of different qualities (e.g. medical grade chitosan, industrial grade chitosan, etc.), provenance (e.g. shrimps, crabs, fungal-based chitosan), degree of DD (60 – 90%) and Mw were characterized and their solubility evaluated in promising imidazole-based ILs. It was demonstrated that especially short-chain ILs in combination with acetate anions possess excellent solubility for all investigated chitosans (Figure 1). From the results of the dissolution tests, promising chitosan-IL combinations were defined for further process development steps.

The preparation of the chitosan-IL spinning dopes (Figure 2, left) was carried out using thermal processing in solids concentrations of up to 8 wt.-% and was monitored and evaluated by rheological investigations as a function of the temperature and shear rate (Figure 2, right). To investigate the stability, processability and spinnability of the homogeneous chitosan-IL-solutions, the spinning dopes were processed into monofilaments on a laboratory scale. In particular, fiber formation was analyzed as a function of the chitosan raw materials and process parameters, such as solid content, temperature, diffusion rate and residence time in the coagulation medium. The obtained results demonstrated, that all investigated chitosan-IL-combinations can be processed into pure chitosan fibers. Therefore, it was successfully proved that ILs are a suitable and promising solvent for the manufacturing of chitosan multifilament yarns.

Wet-spinning of the chitosan multifilament yarns

In the following step, the basic methods developed on the laboratory scale were successfully transferred to a wet-spinning process on a pilot scale. The chitosan multifilament yarns were spun on the wet-spinning plant (Fourné Maschinenbau GmbH) of the ITM. The pilot spinning plant is specially designed for R&D process developments and enables, in particular, test trials with 2 – 60 liters of spinning dope.

For the spinning trials, chitosan-IL spinning dope was first filtered and degassed under specific temperature and pressure conditions. Different spinneret geometries were used for multifilament spinning, including 78 holes of 90 μm (90 µm/78f) and 24 holes of 160 μm (160 µm/12f), respectively. The prepared tempered spinning dope was extruded into a coagulation bath with deionized water as medium. Overall yarn counts of about 50 – 65 tex and filament diameters of about 30 – 50 µm were achieved depending on the spinneret geometry. In order to achieve tailored functionalities, such as high mechanical strength and crystallinity as well as improved molecular orientation, the influence of fiber drawing during the spinning process was systematically investigated. The produced yarns were analyzed for their mechanical and textile-physical properties and compared with conventionally produced acetic acid (AcOH) based chitosan yarns. The DD of the raw material has an important role in this context: a high content of acetamide groups in chitosan with low DD (< 90%) leads to an increase in intermolecular interactions, resulting in improved mechanical properties. The results obtained demonstrate a high functionality as well as significantly improved mechanical properties of the IL spun chitosan multifilament yarns compared to the conventional chitosan fibers (DD 90%) (Figure 3, right). By means of elaborated drawing parameters, tailor-made textile-physical properties, such as elasticity or tensile strength, can be adjusted according to defined requirements.

Textile processing of the chitosan multifilament yarns

During the final phase of the project, the textile processing of the chitosan multifilament yarns from IL into knitted and woven patterns and braids was successfully implemented (Figure 4). The technical processing of conventional chitosan yarns on textile machines has always been a challenge due to insufficient mechanical strength and knot tearing forces. Trouble-free processing in weaving, knitting or braiding processes without special yarn pretreatment or machine adaptations could not be realized so far using conventional chitosan multifilament yarns. In contrast, the chitosan multifilament yarn produced by IL offers sufficient mechanical stability and flexibility to be processed into knitted, woven or braided structures in conventional textile processes on standard industrial production machines. Additional yarn functionalization, such as sizing, further improves the processability of the material and the quality of the finished product.

Acknowledgement

The IGF project 21168 BR of the Research Association Forschungskuratorium Textil e.V. was funded by the Federal Ministry of Economics and Climate Protection via the AiF within the framework of the program for the promotion of joint industrial research (IGF) on the basis of a resolution of the German Bundestag. We would like to thank the above-mentioned institutions for providing the financial resources. Furthermore, we want to thank the member of the ‘Projektbegleitender Ausschuss’ (project accompanying committee) for their support during the project.

The complete publication is available as download.

AutorInnen: Kuznik, Irina; Kruppke, Iris; Cherif, Chokri

Technische Universität Dresden
Fakultät Maschinenwesen
Institut für Textilmaschinen und Textile Hochleistungswerkstofftechnik (ITM)
01062 Dresden

https://tu-dresden.de/mw/itm

chitosan multifilament yarns

More entries from TU Dresden, Institut für Textilmaschinen und Textile Hochleistungswerkstofftechnik ITM

05.09.2022

Development of near-net-shape woven, curved profile preforms

Technische Textilien

Zusammenfassung

At the ITM, the simulation-supported development and weaving implementation of integrally manufactured curved profile preforms with requirement-oriented cross-sectional changes along the profile length for the reinforcement of shell-shaped FRP components was carried out in the IGF project 20903 BR (Curved Profile Preforms).

Bericht

At the ITM, the simulation-supported development and weaving implementation of integrally manufactured curved profile preforms with requirement-oriented cross-sectional changes along the profile length for the reinforcement of shell-shaped FRP components was carried out in the IGF project 20903 BR (Curved Profile Preforms).

AutorInnen: Nuss, Dominik Huỳnh, Thị Anh Mỹ Gereke, Thomas Hoffmann, Gerald Cherif, Chokri

Technische Universität Dresden
Fakultät Maschinenwesen
Institut für Textilmaschinen und Textile Hochleistungswerkstofftechnik (ITM)
01062 Dresden

https://tu-dresden.de/mw/itm

More entries from TU Dresden, Institut für Textilmaschinen und Textile Hochleistungswerkstofftechnik ITM